Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Ethyl cyanoformate → Pirolate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Ethyl cyanoformate | HCID 69336 | — |
| 반응물 | 2-Amino-6,7-dimethoxyquinoline-3-carboxamide | HCID 781584 | — |
| 용매 | Benzene | HCID 241 | — |
| 생성물 | Pirolate | HCID 135445830 | — |
반응 단계
Still further, a mixture of 6,7-dimethoxy-2-aminoquinoline-3-carboxamide (0.5 g., 2 millimoles), ethyl cyanoformate (0.43 g., 44 millimiles) and benzene (30 ml.) is refluxed for three days. The mixture is then cooled, filtered and the solid extracted with chloroform. Concentration of the chloroform extract affords the product which is recrystallized from chloroform.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04120962 |
| 출처 데이터셋 | uspto-grants-1978_10 |
| ORD ID | ord-dd5e7d5fefa5458a8f5c20ee8a84d550 |
| 출처 메모 | uspto-grants-1978_10 |