Benzylamine → N,N-Dimethyl-3-[2-[[(phenylmethyl)imino]methyl]phenoxy]propanamine
반응식
[CH3:1][N:2]([CH3:15])[CH2:3][CH2:4][CH2:5][O:6][C:7]1[CH:14]=[CH:13][CH:12]=[CH:11][C:8]=1[CH:9]=O.[CH2:16]([NH2:23])[C:17]1[CH:22]=[CH:21][CH:20]=[CH:19][CH:18]=1>C1(C)C=CC=CC=1>[CH3:1][N:2]([CH3:15])[CH2:3][CH2:4][CH2:5][O:6][C:7]1[CH:14]=[CH:13][CH:12]=[CH:11][C:8]=1[CH:9]=[N:23][CH2:16][C:17]1[CH:22]=[CH:21][CH:20]=[CH:19][CH:18]=1참가 물질
4
실험 절차
A solution of 20.0 g of 2-(3-dimethylaminopropoxy)-benzaldehyde and 10.3 g of benzylamine in 100 ml of toluene is heated at reflux for 1 hour in a procedure described for Example 1. The yield of product is 22.1 g, boiling point 175°-178° C/0.05 mm of Hg.
후처리
- temperatureat reflux for 1 hour in a procedure
출처 및 근거
- ORD 기록
- ord-37b97694ba1848bba94a7fe99df6e7a5
- 출처 데이터셋
- uspto-grants-1978_10
- 특허 번호
- US04122255
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