Hydrochloric Acid → HCID 178479216, 화합물

HRID 1154119노트

반응식

HRID 1154119 반응식
C([NH:4][CH2:5][CH2:6][CH2:7][N:8]1[C:12]([SH:13])=[N:11][N:10]=[N:9]1)(=O)C.[ClH:14]>>[ClH:14].[NH2:4][CH2:5][CH2:6][CH2:7][N:8]1[C:12]([SH:13])=[N:11][N:10]=[N:9]1

참가 물질

3

반응물 2

HCID 313Hydrochloric AcidHCID 178474793HCID 178474793, 화합물

생성물 1

HCID 178479216HCID 178479216, 화합물

실험 절차

A mixture of 1-(3-acetamidopropyl)-1H-tetrazole-5-thiol (85 g) and 6N hydrochloric acid (1 l) was refluxed for 75 minutes under stirring. The reaction mixture was concentrated in vacuo and precipitates were collected by filtration and washed with hexane and diethyl ether to give 1-(3-aminopropyl)-1H-tetrazole-5-thiol hydrochloride (67.15 g).

후처리

  1. temperaturewas refluxed for 75 minutes
  2. concentrationThe reaction mixture was concentrated in vacuo
  3. customprecipitates
  4. filtrationwere collected by filtration
  5. washwashed with hexane and diethyl ether

출처 및 근거

ORD 기록
ord-e626872f8af34a81917dbcb23313e739
출처 데이터셋
uspto-grants-1984_12
특허 번호
US04487767

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