Sodium Carbonate → alpha-(5-Indenoxy)acetophenone

HRID 1154762

반응식

HRID 1154762 반응식
[OH:1][C:2]1[CH:3]=[C:4]2[C:8](=[CH:9][CH:10]=1)[CH2:7][CH2:6][CH2:5]2.Cl[CH2:12][C:13]([C:15]1[CH:20]=[CH:19][CH:18]=[CH:17][CH:16]=1)=[O:14].C(=O)([O-])[O-].[Na+].[Na+]>C1C=CC=CC=1>[CH2:7]1[C:8]2[C:4](=[CH:3][C:2]([O:1][CH2:12][C:13]([C:15]3[CH:20]=[CH:19][CH:18]=[CH:17][CH:16]=3)=[O:14])=[CH:10][CH:9]=2)[CH:5]=[CH:6]1

참가 물질

5

반응물 3

HCID 10340Sodium CarbonateHCID 107572-ChloroacetophenoneHCID 151185-Indanol

생성물 1

HCID 20563333alpha-(5-Indenoxy)acetophenone

시약·촉매·용매 1

HCID 241Benzene용매

실험 절차

Using the method of Example 1, step A, 5-hydroxyindane is reacted with α-chloroacetophenone in benzene in the presence of sodium carbonate to provide α-(5-indenoxy)acetophenone as a yellow solid.

출처 및 근거

ORD 기록
ord-3f7fc3cc0276422f8629533646612eee
출처 데이터셋
uspto-grants-1981_11
특허 번호
US04298532

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