Isobutyric Acid → Methylthiomethyl Isobutyrate

HRID 1155720노트

반응식

[C:1]([OH:6])(=[O:5])[CH:2]([CH3:4])[CH3:3].[CH3:7][S:8][CH2:9]Cl.C(N(CC)CC)C>>[C:1]([O:6][CH2:7][S:8][CH3:9])(=[O:5])[CH:2]([CH3:4])[CH3:3]

참가 물질

반응물 3

HCID 6590Isobutyric Acid

HCID 8471Triethylamine

HCID 16916Chloromethyl methyl sulfide

생성물 1

HCID 20481371Methylthiomethyl Isobutyrate

실험 절차

This product was prepared according to the procedure described in Example 1, by reacting isobutyric acid with chloromethyl methyl sulfide in the presence of one equivalent of triethylamine; b.p. 64° C./12 mm Hg, nD20 1.4470.

후처리

customThis product was prepared

출처 및 근거

ORD 기록: ord-bd3e082e8ecd4a479789601898ea790b
출처 데이터셋: uspto-grants-1982_06
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US04332829

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