Acrylonitrile → HCID 20536718, 화합물

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[C:1]([CH2:3][CH2:4][O:5][CH:6]([CH3:10])[CH2:7][CH2:8][OH:9])#[N:2].[CH2:11](O)[CH2:12][CH:13]([OH:15])C.C(#N)C=C>>[C:13]([O:9][CH2:8][CH2:7][CH:6]([O:5][CH2:4][CH2:3][C:1]#[N:2])[CH3:10])(=[O:15])[CH:12]=[CH2:11]

참가 물질

반응물 3

HCID 7855Acrylonitrile

HCID 78961,3-Butanediol

HCID 20536719HCID 20536719, 화합물

생성물 1

HCID 20536718HCID 20536718, 화합물

실험 절차

Following the procedures described in Example 1, 3-(2-cyanoethoxy)-1-butanol (bp 145°-150° C./2.5 mm Hg) is prepared from 1,3-butanediol and acrylonitrile, acrylation of which gives the desired product.

출처 및 근거

ORD 기록: ord-0b17e1faaef4466bb60c2699eafb8c46
출처 데이터셋: uspto-grants-1982_06
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US04333963

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