Diethyl Ether → 2,3-Dimethyl-2-aminobutyronitrile hydrochloride

HRID 1156229

반응식

HRID 1156229 반응식
[C-:1]#[N:2].[K+].[CH3:4][CH:5]([CH3:9])[C:6](=O)[CH3:7].[Cl-:10].[NH4+:11].CCOCC>O>[ClH:10].[CH3:7][C:6]([NH2:11])([CH:5]([CH3:9])[CH3:4])[C:1]#[N:2]

참가 물질

6

반응물 4

HCID 3283Diethyl EtherHCID 9032Potassium CyanideHCID 112513-Methyl-2-butanoneHCID 25517Ammonium Chloride

생성물 1

HCID 129454442,3-Dimethyl-2-aminobutyronitrile hydrochloride

시약·촉매·용매 1

HCID 962Water용매

실험 절차

The reactant 2,3-dimethyl-2-aminobutyronitrile hydrochloride was prepared by the following reaction. A solution of 136 grams (g) (2.1 moles) of potassium cyanide in 220 milliliters (ml) of water was added dropwise at 10°-15° C. to a mixture of 172.2 g (2.0 moles) of 3-methyl-2-butanone, 110.2 g (2.1 moles) ammonium chloride, and 300 ml of ether. The mixture was allowed to reach room temperature at which it was stirred overnight.

후처리

  1. customto reach room temperature at which it

출처 및 근거

ORD 기록
ord-51f7cd9ddd6e409594d72f31125435f6
출처 데이터셋
uspto-grants-1982_06
특허 번호
US04335053

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