P-Toluic Acid → 4-Methylbenzoyl Chloride

반응식

[CH3:1][C:2]1[CH:10]=[CH:9][C:5]([C:6](O)=[O:7])=[CH:4][CH:3]=1.S(Cl)([Cl:13])=O>>[CH3:1][C:2]1[CH:10]=[CH:9][C:5]([C:6]([Cl:13])=[O:7])=[CH:4][CH:3]=1

참가 물질

반응물 2

HCID 7470P-Toluic Acid

HCID 24386Thionyl Chloride

생성물 1

HCID 134054-Methylbenzoyl Chloride

실험 절차

4-Methylbenzoyl chloride was prepared in a conventional manner from 4-methylbenzoic acid and thionyl chloride and after excess thionyl chloride was distilled off, was used as the crude product in the side chain chlorination.

후처리

distillationafter excess thionyl chloride was distilled off

출처 및 근거

ORD 기록: ord-4c3ca7fee7ca4cb68a75ae1c5be3919e
출처 데이터셋: uspto-grants-1998_03
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US05723613

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