Pyrrole → 1-[(3-Bromo-2-thienyl)sulfonyl]-1H-pyrrole

HRID 1166946노트

반응식

[Br:1][C:2]1[CH:6]=[CH:5][S:4][C:3]=1[S:7](Cl)(=[O:9])=[O:8].[NH:11]1[CH:15]=[CH:14][CH:13]=[CH:12]1>>[Br:1][C:2]1[CH:6]=[CH:5][S:4][C:3]=1[S:7]([N:11]1[CH:15]=[CH:14][CH:13]=[CH:12]1)(=[O:9])=[O:8]

참가 물질

반응물 2

HCID 8027Pyrrole

HCID 136755983-Bromothiophene-2-sulfonyl chloride

생성물 1

HCID 234455281-[(3-Bromo-2-thienyl)sulfonyl]-1H-pyrrole

실험 절차

N-(3-bromothiophene-2-sulfonyl)pyrrole was prepared in the same manner as described in Example 33A by reacting 3-bromothiophene-2-sulfonylchloride with pyrrole (for 16 hr.). N-(3-bromothiophene-2-sulfonyl)pyrrole was obtained in 54% yield.

후처리

customN-(3-bromothiophene-2-sulfonyl)pyrrole was prepared in the same manner

출처 및 근거

ORD 기록: ord-c880c4f0a2b742cead23a1a9d9a04eb5
출처 데이터셋: uspto-grants-2003_09
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US06613804B2

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