Hydrochloric Acid → 2-Propylthiazolo[4,5-c]quinolin-4-amine hydrochloride

HRID 1168796노트

반응식

HRID 1168796 반응식
[CH2:1]([C:4]1[S:5][C:6]2[C:15]3[CH:14]=[CH:13][CH:12]=[CH:11][C:10]=3[N:9]=[C:8]([NH2:16])[C:7]=2[N:17]=1)[CH2:2][CH3:3].[ClH:18]>>[ClH:18].[CH2:1]([C:4]1[S:5][C:6]2[C:15]3[CH:14]=[CH:13][CH:12]=[CH:11][C:10]=3[N:9]=[C:8]([NH2:16])[C:7]=2[N:17]=1)[CH2:2][CH3:3]

참가 물질

3

반응물 2

HCID 313Hydrochloric AcidHCID 101987192-propylthiazolo[4,5-c]quinolin-4-amine

생성물 1

HCID 226482952-Propylthiazolo[4,5-c]quinolin-4-amine hydrochloride

실험 절차

Using the general method of Example 10, 2-propylthiazolo[4,5-c]quinolin4-amine (1.75 g) was reacted with 1 equivalent of concentrated hydrochloric acid to provide 2-propylthiazolo[4,5-c]quinolin-4-amine hydrochloride as an off-white crystalline solid, m.p. 234-237° C. Analysis: Calculated for C13H13N3S HCl: %C, 55.81; %H, 5.04; %N, 15.02; Found: %C, 55.86; %H, 5.02; %N, 14.99.

출처 및 근거

ORD 기록
ord-9410e60b039c4915a306a1aa44c15bea
출처 데이터셋
uspto-grants-2003_09
특허 번호
US06627640B2

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