Oxalyl chloride → HCID 86054523, 화합물
반응식
[I:1][C:2]1[CH:7]=[CH:6][C:5]([CH2:8][OH:9])=[C:4]([O:10][CH2:11][CH2:12][CH3:13])[CH:3]=1.C(Cl)(=O)C(Cl)=O>CS(C)=O>[I:1][C:2]1[CH:7]=[CH:6][C:5]([CH:8]=[O:9])=[C:4]([O:10][CH2:11][CH2:12][CH3:13])[CH:3]=1참가 물질
4
실험 절차
The procedure is the same as that described above, using 5.5 g, that is 18.8 mmol, of (4-iodo-2-propoxyphenyl)methanol, 1.8 ml of oxalyl chloride and 3 ml of DMSO. After evaporation of the solvents, 5.5 g (100%) of the expected compound are recovered in the form of a yellow solid.
후처리
- customAfter evaporation of the solvents, 5.5 g (100%) of the expected compound
- customare recovered in the form of a yellow solid
출처 및 근거
- ORD 기록
- ord-bdfa82decdb048e99081fb8e363156a0
- 출처 데이터셋
- uspto-grants-2010_11
- 특허 번호
- US07829588B2
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