Lithium hydroxide, monohydrate → HCID 18409065, 화합물

HRID 1174214노트

반응식

HRID 1174214 반응식
[CH3:1][C:2]1[N:7]=[CH:6][C:5]([O:8][CH2:9][C:10]([O:12]CC)=[O:11])=[CH:4][CH:3]=1.O.[OH-].[Li+]>C1COCC1.O>[CH3:1][C:2]1[N:7]=[CH:6][C:5]([O:8][CH2:9][C:10]([OH:12])=[O:11])=[CH:4][CH:3]=1

참가 물질

5

반응물 2

HCID 168937Lithium hydroxide, monohydrateHCID 4614663SLQPGPDBDCSQMM-UHFFFAOYSA-N

생성물 1

HCID 18409065HCID 18409065, 화합물

시약·촉매·용매 2

HCID 962Water용매HCID 8028Tetrahydrofuran용매

반응 조건

온도
25 °C

실험 절차

A solution containing ethyl 6-methyl-3-pyridyloxyacetate (0.026 g, 0.13 mmol) in a mixture of THF (0.5 mL) and water (0.5 mL) was treated with lithium hydroxide monohydrate (0.008 g, 0.19 mmol), stirred at 25° C. for 18 hours, aid concentrated to give the crude product, which was used without purification.

후처리

  1. concentrationaid concentrated

출처 및 근거

ORD 기록
ord-edaf472e97534fa7ac18fb1122352eec
출처 데이터셋
uspto-grants-2010_11
특허 번호
US07834043B2

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