Acetic Acid → HCID 74019072, 화합물

HRID 1175799

반응식

HRID 1175799 반응식
Cl.[CH3:2][O:3][C:4]1[CH:5]=[C:6]([NH:10][NH2:11])[CH:7]=[CH:8][CH:9]=1.[N+:12]([CH2:15][C:16]([C:18]1C=CC=C[CH:19]=1)=O)([O-:14])=[O:13].[C:24]([O-])(=O)[CH3:25].[Na+].[C:29](O)(=O)[CH3:30]>O>[CH3:2][O:3][C:4]1[CH:5]=[C:6]([NH:10][N:11]=[C:29]([C:24]2[CH:25]=[CH:19][CH:18]=[CH:16][C:15]=2[N+:12]([O-:14])=[O:13])[CH3:30])[CH:7]=[CH:8][CH:9]=1

참가 물질

6

반응물 4

HCID 176Acetic AcidHCID 948332-Nitro-1-phenylethanoneHCID 517045Sodium AcetateHCID 27239403-Methoxyphenylhydrazine hydrochloride

생성물 1

HCID 74019072HCID 74019072, 화합물

시약·촉매·용매 1

HCID 962Water용매

실험 절차

A mixture of 3-methoxyphenylhydrazine hydrochloride (1.75 g), 2-nitroacetophenone (1.65 g), sodium acetate (0.82 g) and acetic acid (10 ml) was stirred at room temperature for 4 days. To the reaction mixture was added water, extracted with ethyl acetate. The extract was washed with water, brine, dried over anhydrous magnesium sulfate. The solvent was distilled off under reduced pressure to obtain the target compound (2.72 g).

후처리

  1. extractionextracted with ethyl acetate
  2. washThe extract was washed with water, brine
  3. dry with materialdried over anhydrous magnesium sulfate
  4. distillationThe solvent was distilled off under reduced pressure

출처 및 근거

ORD 기록
ord-573261e1a46940b09dc4e699d60da9d2
출처 데이터셋
uspto-grants-2010_11
특허 번호
US07842701B2

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