4-Morpholinecarbonyl chloride → HCID 10150335, 화합물

HRID 1179774노트

반응식

HRID 1179774 반응식
[Cl:1][C:2]1[CH:3]=[N:4][CH:5]=[C:6]([Cl:16])[C:7]=1[O:8][C:9]1[CH:14]=[CH:13][C:12]([OH:15])=[CH:11][CH:10]=1.[N:17]1([C:23](Cl)=[O:24])[CH2:22][CH2:21][O:20][CH2:19][CH2:18]1>>[Cl:16][C:6]1[CH:5]=[N:4][CH:3]=[C:2]([Cl:1])[C:7]=1[O:8][C:9]1[CH:10]=[CH:11][C:12]([O:15][C:23]([N:17]2[CH2:22][CH2:21][O:20][CH2:19][CH2:18]2)=[O:24])=[CH:13][CH:14]=1

참가 물질

3

반응물 2

HCID 848104-Morpholinecarbonyl chlorideHCID 27265874-(3,5-Dichloro-pyridin-4-yloxy)-phenol

생성물 1

HCID 10150335HCID 10150335, 화합물

실험 절차

The title compound was prepared from 4-(3,5-dichloro-pyridin-4-yloxy)-phenol and morpholine-4-carbonyl chloride. The crude product was purified by preparative HPLC (66%, white crystals. HPLC-MS m/z=368.9 (M+1), Rt: 4.0 min.

후처리

  1. customThe crude product was purified by preparative HPLC (66%, white crystals

출처 및 근거

ORD 기록
ord-efe6ce4021164b7fb6245eba4599bdb8
출처 데이터셋
uspto-grants-2007_10
특허 번호
US07279470B2

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