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Sodium Hydroxide → 2-(2,4-dimethoxyphenyl)-4,5-dihydro-thiazole-4-(R)-carboxylic acid

HRID 1181633
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HRID 1181633 반응식
C([O:3][C:4]([C@@H:6]1[CH2:10][S:9][C:8]([C:11]2[CH:16]=[CH:15][C:14]([O:17][CH3:18])=[CH:13][C:12]=2[O:19][CH3:20])=[N:7]1)=[O:5])C.[OH-].[Na+]>C(OC)(C)(C)C>[CH3:20][O:19][C:12]1[CH:13]=[C:14]([O:17][CH3:18])[CH:15]=[CH:16][C:11]=1[C:8]1[S:9][CH2:10][C@@H:6]([C:4]([OH:5])=[O:3])[N:7]=1
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참가 물질

4

반응물 2

HCID 14798Sodium HydroxideHCID 17747724ethyl-2-(2,4-dimethoxyphenyl)-4,5-dihydro-thiazole-4-(R)-carboxylate

생성물 1

HCID 177477252-(2,4-dimethoxyphenyl)-4,5-dihydro-thiazole-4-(R)-carboxylic acid

시약·촉매·용매 1

HCID 15413tert-Butyl methyl ether용매

실험 절차

Ethyl-2-(2,4-dimethoxyphenyl)-4,5-dihydro-thiazole-4-(R)-carboxylate is refluxed with aqueous sodium hydroxide in methyl tertiary-butyl ether (MTBE) to form 2-(2,4-dimethoxyphenyl)-4,5-dihydro-thiazole-4-(R)-carboxylic acid.

출처 및 근거

ORD 기록
ord-51617e526c994f5abfe351460e347d88
출처 데이터셋
uspto-grants-2007_10
DOI
10.6084/m9.figshare.5104873.v1
특허 번호
US07285670B2

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