m-Chloroperbenzoic acid → HCID 86679095, 화합물

HRID 1183476

반응식

HRID 1183476 반응식
[Br:1][C:2]1[CH:7]=[CH:6][CH:5]=[C:4]([S:8][C:9]2[CH:14]=[CH:13][CH:12]=[CH:11][CH:10]=2)[N:3]=1.ClC1C=CC=C(C(OO)=[O:23])C=1>C(Cl)Cl>[C:9]1([S:8]([C:4]2[CH:5]=[CH:6][CH:7]=[C:2]([Br:1])[N:3]=2)=[O:23])[CH:10]=[CH:11][CH:12]=[CH:13][CH:14]=1

참가 물질

4

반응물 2

HCID 70297m-Chloroperbenzoic acidHCID 8245912-Bromo-6-phenylsulfanylpyridine

생성물 1

HCID 86679095HCID 86679095, 화합물

시약·촉매·용매 1

HCID 6344Dichloromethane용매

실험 절차

2-Bromo-6-phenylsulfanyl-pyridine (0.5323 g, 2 mmol) was dissolved in CH2Cl2 (20 mL) and m-chloroperbenzoic acid (0.345 g, 2 mmol) was added. The reaction was stirred at room temperature overnight then submitted to aqueous workup and purification on silica gel to give the title compound.

후처리

  1. customthen submitted to aqueous workup and purification on silica gel

출처 및 근거

ORD 기록
ord-26914c45d55841a4a736b549738cd277
출처 데이터셋
uspto-grants-2014_03
특허 번호
US08664220B2

연결된 노트

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