Phenol → HCID 86664216, 화합물

HRID 1184470노트

반응식

HRID 1184470 반응식
[F:1][C:2]1[CH:9]=[C:8]([OH:10])[C:7]([N+:11]([O-:13])=[O:12])=[CH:6][C:3]=1[CH:4]=[O:5].C1(O)C=CC=CC=1.[CH3:21][O:22][C:23](=[O:27])[CH:24](Br)[CH3:25]>>[F:1][C:2]1[C:3]([CH:4]=[O:5])=[CH:6][C:7]([N+:11]([O-:13])=[O:12])=[C:8]([CH:9]=1)[O:10][CH:24]([CH3:25])[C:23]([O:22][CH3:21])=[O:27]

참가 물질

4

반응물 3

HCID 996PhenolHCID 95576Methyl 2-bromopropionateHCID 866642172-Fluoro-4-hydroxy-5-nitro-benzaldehyde

생성물 1

HCID 86664216HCID 86664216, 화합물

실험 절차

Using 2-fluoro-4-hydroxy-5-nitrobenzaldehyde as the phenol and methyl-2-bromopropanoate as the alkylating agent in the general procedure for alkylation of substituted-2-nitrophenols gives the title compound as a white solid: ESI-MS: m/z 272.1 (M+H)+.

출처 및 근거

ORD 기록
ord-b1f3d70c2d9c42eeb02e26e5aa85d878
출처 데이터셋
uspto-grants-2014_03
특허 번호
US08669249B2

반응 노트

불러오는 중…