Sodium Hydroxide → Undeca-2,4,8-trienoic acid
반응식
[CH:1](=[O:12])[CH:2]=[CH:3][CH:4]=[CH:5][CH2:6][CH2:7][CH:8]=[CH:9][CH2:10][CH3:11].[OH-:13].[Na+]>O.[Ag-]=O>[C:1]([OH:13])(=[O:12])[CH:2]=[CH:3][CH:4]=[CH:5][CH2:6][CH2:7][CH:8]=[CH:9][CH2:10][CH3:11]참가 물질
5
반응 조건
- 온도
- 20 °C
실험 절차
For example, the 2,4,8-undecatrienal is added to a suspension of silver (I) oxide (1.1 eq) in water. The mixture is stirred at 20° C. and 50% sodium hydroxide solution (equal weight to the aldehyde), is added over 30 minutes allowing the batch to exotherm to 60° C. The solution is filtered through celite, and the aqueous filtrate acidified to pH 1 with hydrochloric acid solution, to give 2,4,8-undecatrienoic acid.
후처리
- customto exotherm to 60° C
- filtrationThe solution is filtered through celite
출처 및 근거
- ORD 기록
- ord-749372d48f064457a6708bf563870855
- 출처 데이터셋
- uspto-grants-2006_08
- 특허 번호
- US07098350B2
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