반응식
[C:1]([O:5][C:6]([N:8]1[CH2:20][C@@H:19]([CH3:21])[N:18]2[C@H:10]([CH2:11][C:12]3[C:17]2=[N:16][C:15](Br)=[CH:14][CH:13]=3)[CH2:9]1)=[O:7])([CH3:4])([CH3:3])[CH3:2].[C:23]([O:27]C(N1C[C@@H](C)N2[C@H](CC3C2=NC(O)=CC=3)C1)=O)(C)(C)[CH3:24].[H-].[Na+].C(Br)C>>[C:1]([O:5][C:6]([N:8]1[CH2:20][C@@H:19]([CH3:21])[N:18]2[C@H:10]([CH2:11][C:12]3[C:17]2=[N:16][C:15]([O:27][CH2:23][CH3:24])=[CH:14][CH:13]=3)[CH2:9]1)=[O:7])([CH3:4])([CH3:3])[CH3:2]참가 물질
5
반응물 4
생성물 1
실험 절차
This compound was prepared in analogy to Example 22 intermediate b), from (4R,9aR)-6-hydroxy-4-methyl-3,4,9,9a-tetrahydro-1H-2,4a,5-triaza-fluorene-2-carboxylic acid tert-butyl ester, sodium hydride and ethyl bromide.
출처 및 근거
- ORD 기록
- ord-66a1909896b24caab495aec954787752
- 출처 데이터셋
- uspto-grants-2006_08
- 특허 번호
- US07098337B2
연결된 노트
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