Hydrazine hydrate (1:1) → HCID 21249171, 화합물

HRID 1194674노트

반응식

HRID 1194674 반응식
[CH3:1][S:2][C:3]1[CH:8]=[CH:7][C:6]([C:9](=O)[CH:10]([CH3:15])[CH2:11][C:12](O)=[O:13])=[CH:5][CH:4]=1.O.[NH2:18][NH2:19]>C(O)(C)C>[CH3:1][S:2][C:3]1[CH:8]=[CH:7][C:6]([C:9]2[CH:10]([CH3:15])[CH2:11][C:12](=[O:13])[NH:18][N:19]=2)=[CH:5][CH:4]=1

참가 물질

4

반응물 2

HCID 24654Hydrazine hydrate (1:1)HCID 13693406HCID 13693406, 화합물

생성물 1

HCID 21249171HCID 21249171, 화합물

시약·촉매·용매 1

HCID 3776Isopropanol용매

실험 절차

2.3 g (0.01 mole) of 4-(4-methylthio-phenyl)-4-oxo-3-methyl-butyric acid and 1 ml of hydrazine hydrate are heated under reflux in 20 ml of isopropanol for 2 hour. After the mixture has been cooled, the product is filtered off with suction and dried.

후처리

  1. temperatureAfter the mixture has been cooled
  2. filtrationthe product is filtered off with suction
  3. customdried

출처 및 근거

ORD 기록
ord-fdb03b77d58940cf8d186e5619f473b4
출처 데이터셋
uspto-grants-1989_03
특허 번호
US04816454

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