HCID 19819017, 화합물 → HCID 19819020, 화합물

HRID 1195238노트

반응식

HRID 1195238 반응식
[ClH:1].[CH:2]1([C:5]([CH:7]2[CH2:9][CH2:8]2)=[NH:6])[CH2:4][CH2:3]1>CS(C)=O>[Cl-:1].[N+:6]12[CH2:9][CH2:8][CH2:7][C:5]=1[CH2:2][CH2:3][CH2:4]2

참가 물질

3

반응물 1

HCID 19819017HCID 19819017, 화합물

생성물 1

HCID 19819020HCID 19819020, 화합물수율 55%

시약·촉매·용매 1

HCID 679Dimethyl Sulfoxide용매

반응 조건

온도
100 °C

실험 절차

A solution of dicyclopropylmethanimine hydrochloride (1.00 g, 6.87 mmol) in 6.0 ml of dimethyl sulfoxide was heated with stirring at 100° C. for 4 hours. The solvent was distilled out in vacuo and isobutyl alcohol (6 ml) was added to the residue. Precipitated crystals was obtained and dried in vacuo to afford 0.55 g (Yield: 55%) of the desired compound.

후처리

  1. distillationThe solvent was distilled out in vacuo and isobutyl alcohol (6 ml)
  2. additionwas added to the residue
  3. customPrecipitated crystals
  4. customwas obtained
  5. customdried in vacuo

출처 및 근거

ORD 기록
ord-d0db1dab158242feb1f62fa127826663
출처 데이터셋
uspto-grants-1992_05
특허 번호
US05110945

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