2-Mercaptoethanol → 2-[{3-(1,3-Benzodioxol-5-yl)propyl}dithio]ethanol

HRID 1195294노트

반응식

HRID 1195294 반응식
[O:1]1[C:5]2[CH:6]=[CH:7][C:8]([CH2:10][CH2:11][CH2:12][SH:13])=[CH:9][C:4]=2[O:3][CH2:2]1.[SH:14][CH2:15][CH2:16][OH:17]>>[O:1]1[C:5]2[CH:6]=[CH:7][C:8]([CH2:10][CH2:11][CH2:12][S:13][S:14][CH2:15][CH2:16][OH:17])=[CH:9][C:4]=2[O:3][CH2:2]1

참가 물질

3

반응물 2

HCID 15672-MercaptoethanolHCID 190016193-(1,3-Dioxaindan-5-yl)propane-1-thiol

생성물 1

HCID 190016282-[{3-(1,3-Benzodioxol-5-yl)propyl}dithio]ethanol수율 43.8%

실험 절차

8.4 g of the title compound was prepared from 27.8 g of 3-(1,3-benzodioxol-5-yl)propanethiol and 5.5 g of 2-mercaptoethanol as a colorless oil according to the same procedure as that described in Example 1.

출처 및 근거

ORD 기록
ord-210d9daad1034a6e956db964740c89d9
출처 데이터셋
uspto-grants-1992_05
특허 번호
US05110956

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