Benzoyl Peroxide → HCID 14368704, 화합물
반응식
[F:1][C:2]1[CH:11]=[C:10]([F:12])[CH:9]=[C:8]2[C:3]=1[CH:4]=[CH:5][CH:6]=[C:7]2[CH3:13].[Br:14]N1C(=O)CCC1=O.C(OOC(=O)C1C=CC=CC=1)(=O)C1C=CC=CC=1>C(Cl)(Cl)(Cl)Cl>[F:1][C:2]1[CH:11]=[C:10]([F:12])[CH:9]=[C:8]2[C:3]=1[CH:4]=[CH:5][CH:6]=[C:7]2[CH2:13][Br:14]참가 물질
5
실험 절차
1.35 g of 5,7-Difluoro-1-methylnaphthaline in 10 ml of carbon tetrachloride are refluxed for 41/2 hours with 1.4 g of N-bromosuccinimide and 50 mg of dibenzoylperoxide. The cooled mixture is filtered and the solvent removed under vacuum. The purity of the crystalline crude product is sufficient for further reaction, m.p. 74°-76.5°.
후처리
- filtrationThe cooled mixture is filtered
- customthe solvent removed under vacuum
- customThe purity of the crystalline crude product is sufficient for further reaction, m.p. 74°-76.5°
출처 및 근거
- ORD 기록
- ord-8c79336066a24a918e8010e041886d60
- 출처 데이터셋
- uspto-grants-1992_05
- 특허 번호
- US05112851
반응 노트
불러오는 중…