Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
1-(4'-Methoxy(1,1'-biphenyl)-4-yl)ethanone → 4'-Methoxy(1,1'-biphenyl)-4-carboxylic acid
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 1-(4'-Methoxy(1,1'-biphenyl)-4-yl)ethanone | HCID 301557 | — |
| 반응물 | Sodium hypobromite | HCID 23673712 | — |
| 용매 | 1,4-Dioxane | HCID 31275 | — |
| 생성물 | 4'-Methoxy(1,1'-biphenyl)-4-carboxylic acid | HCID 2759552 | 90% |
반응 단계
A solution of 18 g of 4-acetyl-4'-methoxybiphenyl in 285 ml of dioxane was oxidized with a dilute sodium hypobromite. Recrystallization from ethanol and acetic acid gave 4'-methoxybiphenyl-4-carboxylic acid melting at 285° C.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05114613 |
| 출처 데이터셋 | uspto-grants-1992_05 |
| ORD ID | ord-815353fc731c4aa0a12ab6f1fe7a78a7 |
| 출처 메모 | uspto-grants-1992_05 |