Bromide ion → 2-Bromo-1,1-diethoxypropane
반응식
[CH2:1]([O:3][CH:4]([O:7][CH2:8][CH3:9])[CH2:5][CH3:6])[CH3:2].[Br-:10]>C(Cl)(Cl)(Cl)Cl>[CH2:1]([O:3][CH:4]([O:7][CH2:8][CH3:9])[CH:5]([Br:10])[CH3:6])[CH3:2]참가 물질
4
실험 절차
13.22 g of propion-aldehyde-diethyl-acetal are dissolved in 15 ml of carbon tetrachloride; at -10° C. 20 ml of the carbon tetrachloride solution of 17.58 g of bromide are dropped to it under stirring. After its warming to room temperature it is distilled in vacuo.
후처리
- customat -10° C
- distillationis distilled in vacuo
출처 및 근거
- ORD 기록
- ord-0eb4831cd9d74c588e59ab30b8a74767
- 출처 데이터셋
- uspto-grants-1992_05
- 특허 번호
- US05116402
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