Titanium → Neodymium titanium oxide (Nd2Ti2O7)

HRID 1196816

반응식

HRID 1196816 반응식
[OH2:1].O.O.O.C([O-])(=[O:7])C.[Nd+3:9].C([O-])(=[O:12])C.C([O-])(=[O:16])C.[NH4+].C([O-])(=O)C(C)[OH:21].[Ti:25]>>[O-2:7].[O-2:12].[O-2:16].[O-2:21].[O-2:1].[O-2:7].[O-2:7].[Ti+4:25].[Ti+4:25].[Nd+3:9].[Nd+3:9]

참가 물질

4

반응물 3

HCID 23963TitaniumHCID 62358Ammonium LactateHCID 131717395Neodymium acetate tetrahydrate

생성물 1

HCID 166010Neodymium titanium oxide (Nd2Ti2O7)

반응 조건

온도
99 °C

실험 절차

Neodymium titanate (Nd2O3.2TiO2) was prepared as follows. Neodymium acetate tetrahydrate (169.7 g, 0.50 mole) and Tyzor®-LA (290.3 g, 0.50 mole) were charged to a 500 ml flask under a nitrogen atmosphere. Tyzor®-LA is a 50% aqueous solution of the lactic acid ammonium salt of chelated titanium manufactured by E.I. du Pont de Nemours and Co., Wilmington, Del. ("Du Pont Co."). The charge was heated to reflux (99° C.) and maintained at reflux for about 30 mins. The temperature of the violet-colored solution was then adjusted to 80°-85° C.

후처리

  1. temperatureThe charge was heated
  2. temperaturemaintained
  3. temperatureat reflux for about 30 mins
  4. customwas then adjusted to 80°-85° C.

출처 및 근거

ORD 기록
ord-d6d46cb4c13243b39ca04af3c931dd3e
출처 데이터셋
uspto-grants-1992_05
특허 번호
US05116790

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