Pyrilamine hydrochloride → Pyrilamine

HRID 1197477

반응식

HRID 1197477 반응식
[CH3:1][N:2]([CH2:4][CH2:5][N:6]([C:16]1[CH:17]=[CH:18][CH:19]=[CH:20][N:21]=1)[CH2:7][C:8]1[CH:9]=[CH:10][C:11]([O:14][CH3:15])=[CH:12][CH:13]=1)[CH3:3].Cl>O>[CH3:1][N:2]([CH2:4][CH2:5][N:6]([C:16]1[CH:17]=[CH:18][CH:19]=[CH:20][N:21]=1)[CH2:7][C:8]1[CH:13]=[CH:12][C:11]([O:14][CH3:15])=[CH:10][CH:9]=1)[CH3:3]

참가 물질

3

반응물 1

HCID 80139Pyrilamine hydrochloride2회

생성물 1

HCID 4992Pyrilamine수율 99.5%

시약·촉매·용매 1

HCID 962Water용매

실험 절차

A second solution of antihistamine was prepared by dissolving 1.52 grams of the pyrilamine HCl in 60 ml of purified water. The molecular weight of the pyrilamine hydrochloride is 321.9 which resulted in an aqueous solution of 4.7×10-3 moles of pyrilamine. The pH of the solution was adjusted to 7.4 with Na2HPO4 ·7H2O.

후처리

  1. customA second solution of antihistamine was prepared

출처 및 근거

ORD 기록
ord-7a27fe42fd3640e187b42e3d8cb4884e
출처 데이터셋
uspto-grants-1994_01
특허 번호
US05276044

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