Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Potassium Carbonate → HCID 178418677, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Potassium Carbonate | HCID 11430 | — |
| 반응물 | 4-Butoxy-2,3-difluorophenol | HCID 19103433 | — |
| 반응물 | HCID 178444389 | HCID 178444389 | — |
| 용매 | Dimethylformamide | HCID 6228 | — |
| 생성물 | HCID 178418677 | HCID 178418677 | — |
반응 단계
0.1 mol of 2,3-difluoro-4-butoxyphenol, 0.11 mol of trans-4-pentylcyclohexylmethyl bromide and 0.11 mol of potassium carbonate are heated at 100° in 100 ml of dimethylformamide (DMF) for 16 hours. After cooling, the inorganic salts are filtered off with suction, the filtrate is concentrated and water is added. Extraction with methylene chloride gives 1-butoxy-2,3-difluoro-4-(trans-4-pentylcyclohexylmethoxy)benzene.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05279764 |
| 출처 데이터셋 | uspto-grants-1994_01 |
| ORD ID | ord-1bae8b3220744c4abf0f5bfe7aab8377 |
| 출처 메모 | uspto-grants-1994_01 |