Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Sodium borohydride → trans-3-[2-(7-Chloroquinolin-2-yl)ethenyl]benzyl alcohol
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Sodium borohydride | HCID 4311764 | — |
| 반응물 | 3-[(E)-2-(7-Chloroquinolin-2-yl)ethenyl]benzaldehyde | HCID 10017305 | — |
| 용매 | Methanol | HCID 887 | — |
| 생성물 | trans-3-[2-(7-Chloroquinolin-2-yl)ethenyl]benzyl alcohol | HCID 10827738 | — |
반응 단계
Solid sodium borohydride (2.5 g) was added in portions to a stirred suspension of crude 3-[2(E)-(7-chloroquinolin-2-yl)ethenyl]benzaldehyde (5.8 g) in methanol (200 ml). The mixture was filtered and the filtrate was concentrated to ca 70 ml and diluted with hot water to give crystals, m.p. 141° C.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05281593 |
| 출처 데이터셋 | uspto-grants-1994_01 |
| ORD ID | ord-79408cb9ec7d4ae1be7b3f1d54a7a93c |
| 출처 메모 | uspto-grants-1994_01 |