Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
m-Chloroperbenzoic acid → N-tert-Butyl-a-phenylnitrone
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | m-Chloroperbenzoic acid | HCID 70297 | — |
| 반응물 | N-(1,1-Dimethylethyl)benzenemethanamine | HCID 76908 | — |
| 용매 | Dichloromethane | HCID 6344 | — |
| 생성물 | N-tert-Butyl-a-phenylnitrone | HCID 4390 | — |
반응 단계
Following the general procedure of Example 1, N-benzyl-N-tert-butylamine is oxidized using a solution of 3-chloroperoxybenzoic acid dissolved in methylene chloride to give N-tert-butyl-alpha-phenyl nitrone as a white solid melting at 70°-72° C. This is the nitrone described in Japanese Sho No. 59-11345.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04898901 |
| 출처 데이터셋 | uspto-grants-1990_02 |
| ORD ID | ord-4cea29d3563046168c242b9deb9efc7b |
| 출처 메모 | uspto-grants-1990_02 |