Hexylamine → 2,2,2-Trifluoro-n-hexylacetamide

HRID 1199282노트

반응식

HRID 1199282 반응식
[F:1][C:2]([F:9])([F:8])[C:3]([O:5]CC)=O.[CH2:10]([NH2:16])[CH2:11][CH2:12][CH2:13][CH2:14][CH3:15]>>[CH2:10]([NH:16][C:3](=[O:5])[C:2]([F:1])([F:8])[F:9])[CH2:11][CH2:12][CH2:13][CH2:14][CH3:15]

참가 물질

3

반응물 2

HCID 8102HexylamineHCID 9794Ethyl trifluoroacetate

생성물 1

HCID 5394242,2,2-Trifluoro-n-hexylacetamide

실험 절차

In a manner similar to Example 6, ethyl trifluoroacetate (131 g, 0.92 m) was reacted with n-hexylamine. The resulting amide distilled at 64° C./0.2 mm Hg and amounted to 154 g.

후처리

  1. distillationThe resulting amide distilled at 64° C./0.2 mm Hg

출처 및 근거

ORD 기록
ord-3acd5797c63a4ed1a6f577ca9fca6167
출처 데이터셋
uspto-grants-1990_02
특허 번호
US04899249

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