홈MCP워크벤치Skills
홈워크벤치알림마이페이지
llms.txt · MCP 가이드개인정보처리방침 · 이용약관 · 지원v1.8.0
  1. 홈
  2. /반응

Hydrochloric Acid → HCID 178476419, 화합물

HRID 1199724
노트
인쇄 미리보기

반응식

HRID 1199724 반응식
[C:1]([O:4][CH2:5][CH2:6][O:7][C:8]1[CH:21]=[CH:20][C:19]2[O:18][C:17]3[C:12](=[CH:13][CH:14]=[C:15]([C:22]#[N:23])[CH:16]=3)[C:11](=[O:24])[C:10]=2[CH:9]=1)(=[O:3])[CH3:2].[N-:25]=[N+:26]=[N-:27].[Na+].[Cl-].[NH4+].Cl>CN(C)C=O>[C:1]([O:4][CH2:5][CH2:6][O:7][C:8]1[CH:21]=[CH:20][C:19]2[O:18][C:17]3[C:12](=[CH:13][CH:14]=[C:15]([C:22]4[NH:27][N:26]=[N:25][N:23]=4)[CH:16]=3)[C:11](=[O:24])[C:10]=2[CH:9]=1)(=[O:3])[CH3:2]
참가 물질실험 절차후처리출처 및 근거반응 노트

참가 물질

6

반응물 4

HCID 313Hydrochloric AcidHCID 25517Ammonium ChlorideHCID 33557Sodium AzideHCID 198655172-[(6-Cyano-9-oxo-9H-xanthen-2-yl)oxy]ethyl acetate

생성물 1

HCID 178476419HCID 178476419, 화합물

시약·촉매·용매 1

HCID 6228Dimethylformamide용매

실험 절차

The cyanoxanthone from step (B) (2.9 g), sodium azide (0.61 g), ammonium chloride (0.53 g) and dimethylformamide (50 ml) were heated together at 125° for 8 h. The reaction mixture was poured into an iced aqueous solution of hydrochloric acid (excess) and the product filtered off and dried. Recrystallisation from dimethylformamide yielded the title compound, m.p. 216°-218° C.

후처리

  1. filtrationthe product filtered off
  2. customdried
  3. customRecrystallisation from dimethylformamide

출처 및 근거

ORD 기록
ord-ffda02a935a54adf9b690b8124af81ca
출처 데이터셋
uspto-grants-1990_02
DOI
10.6084/m9.figshare.5104873.v1
특허 번호
US04902701

반응 노트

불러오는 중…

이 페이지에서참가 물질실험 절차후처리출처 및 근거반응 노트