Hydrochloric Acid → HCID 14328079, 화합물
반응식
[C:1]1([CH2:7][CH2:8][CH2:9][NH:10][C:11]2[CH:20]=[CH:19][C:14]3[NH:15][C:16](=[O:18])[O:17][C:13]=3[CH:12]=2)[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.[ClH:21]>CO>[ClH:21].[C:1]1([CH2:7][CH2:8][CH2:9][NH:10][C:11]2[CH:20]=[CH:19][C:14]3[NH:15][C:16](=[O:18])[O:17][C:13]=3[CH:12]=2)[CH:2]=[CH:3][CH:4]=[CH:5][CH:6]=1참가 물질
4
실험 절차
A methanol solution (40 ml) containing 3.06 g of 6-(3-Phenylpropylamino)-2-benzoxazolone was combined with an ethereal solution saturated with gaseous hydrogen chloride (40 ml) at ice-bath temperature. The resulting solid was collected by filtration, washed with ether and dried to give the title compound (3.470 g).
후처리
- filtrationThe resulting solid was collected by filtration
- washwashed with ether
- customdried
출처 및 근거
- ORD 기록
- ord-48b32ce60b624fd98ed44c4226548a80
- 출처 데이터셋
- uspto-grants-1990_02
- 특허 번호
- US04904685
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