Hydrochloric Acid → HCID 22063499, 화합물

HRID 12101노트

반응식

[F:1][C:2]1[CH:7]=[CH:6][C:5]([CH2:8][C:9]([NH:12]C=O)([CH3:11])[CH3:10])=[C:4]([CH3:15])[CH:3]=1.Cl>>[F:1][C:2]1[CH:7]=[CH:6][C:5]([CH2:8][C:9]([NH2:12])([CH3:10])[CH3:11])=[C:4]([CH3:15])[CH:3]=1

참가 물질

반응물 2

HCID 313Hydrochloric Acid

HCID 22063470HCID 22063470, 화합물

생성물 1

HCID 22063499HCID 22063499, 화합물

실험 절차

In order to prepare the amine, 27.0 g (130 mmol) of N-[2-(4-fluoro-2-methylphenyl)-1,1-dimethylethyl]formamide is reacted as described in the method for Example 10(c). White solid. Yield: 15.5 g (55%, hydrochloride); melting point: 277° C.-280° C.

후처리

customis reacted

출처 및 근거

ORD 기록: ord-2f2ca50b285c466c8332057972630786
출처 데이터셋: uspto-grants-2010_06
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US07727984B2

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