Dimethylformamide dimethyl acetal → HCID 21939863, 화합물

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CO[CH:3](OC)[N:4]([CH3:6])[CH3:5].[C:9]([NH:12][C:13]1[CH:14]=[C:15]2[C:19](=[CH:20][CH:21]=1)[C:18](=[O:22])[CH2:17][CH2:16]2)(=[O:11])[CH3:10]>>[CH3:3][N:4](/[CH:6]=[C:17]1/[C:18](=[O:22])[C:19]2[C:15]([CH2:16]/1)=[CH:14][C:13]([NH:12][C:9](=[O:11])[CH3:10])=[CH:21][CH:20]=2)[CH3:5]

참가 물질

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HCID 78373Dimethylformamide dimethyl acetal

HCID 312894N1-(1-oxo-2,3-dihydro-1H-inden-5-yl)acetamide

생성물 1

HCID 21939863HCID 21939863, 화합물

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온도: 100 °C

실험 절차

Dimethylformamide dimethylacetal was added to 5-acetamido-1-indanone (2.5 g, 13.2 mmol), which was stirred at 100° C. for 3.5 hours, and cooled to room temperature. The precipitated crude products were collected, which was washed with ethyl acetate to give the titled compound (2.73 g).

후처리

temperaturecooled to room temperature
customThe precipitated crude products
customwere collected
washwhich was washed with ethyl acetate

출처 및 근거

ORD 기록: ord-8e459ffcea8549cabb7946ba3da3ae7f
출처 데이터셋: uspto-grants-2006_10
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US07115750B1

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