HCID 69585181, 화합물 → HCID 21940439, 화합물

HRID 1243142노트

반응식

HRID 1243142 반응식
C([O:5][C:6]([C:8]1([C:18](=[O:31])[NH:19][C:20]2[CH:25]=[CH:24][C:23]([N:26]([CH2:29][CH3:30])[CH2:27][CH3:28])=[CH:22][CH:21]=2)[CH2:17][CH2:16][C:15]2[C:10](=[CH:11][CH:12]=[CH:13][CH:14]=2)[CH2:9]1)=[O:7])(C)(C)C>Cl.O1CCOCC1>[CH2:29]([N:26]([CH2:27][CH3:28])[C:23]1[CH:22]=[CH:21][C:20]([NH:19][C:18]([C:8]2([C:6]([OH:7])=[O:5])[CH2:17][CH2:16][C:15]3[C:10](=[CH:11][CH:12]=[CH:13][CH:14]=3)[CH2:9]2)=[O:31])=[CH:25][CH:24]=1)[CH3:30]

참가 물질

4

반응물 1

HCID 69585181HCID 69585181, 화합물

생성물 1

HCID 21940439HCID 21940439, 화합물

시약·촉매·용매 2

HCID 313Hydrochloric Acid용매HCID 312751,4-Dioxane용매

실험 절차

The t-butyl ester from Example 16A was dissolved in 4 N HCl in dioxane (1.0 mL) and the resulting mixture was stirred at ambient temperature for 4 hours. The mixture was concentrated under reduced pressure to provide the titled compound.

후처리

  1. concentrationThe mixture was concentrated under reduced pressure

출처 및 근거

ORD 기록
ord-5b068b07cb9c49ab8edc6ffb2793eebc
출처 데이터셋
uspto-grants-2006_10
특허 번호
US07115767B2

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