Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Glycolic Acid → HCID 178423363, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Glycolic Acid | HCID 757 | — |
| 반응물 | Thionyl Chloride | HCID 24386 | — |
| 반응물 | 6-Methylpyridine-2,3-diamine | HCID 2734420 | — |
| 용매 | Chloroform | HCID 6212 | — |
| 생성물 | HCID 178423363 | HCID 178423363 | — |
반응 단계
In accordance with scheme 4, a corresponding 2,3-diamino-6-methyl pyridine (R5=methyl, XV) and glycolic acid were heated at 150° C. for about 1 h. The residue was suspended in chloroform and treated with thionyl chloride for about 4 h. After workup 2-chloromethyl-5-methyl-3H-imidazo[4,5-b]pyridine hydrochloride (XVII) was obtained.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07122545B2 |
| 출처 데이터셋 | uspto-grants-2006_10 |
| ORD ID | ord-d3fa850db4f44546a86a78d9daa1e420 |
| 출처 메모 | uspto-grants-2006_10 |