Glycine ethyl ester → Ethyl 2-(2-hydroxy-3-methoxypropylamino)acetate

HRID 1244787

반응식

HRID 1244787 반응식
[CH3:1][O:2][CH2:3][CH:4]1[O:6][CH2:5]1.[CH2:7]([O:9][C:10](=[O:13])[CH2:11][NH2:12])[CH3:8]>C(O)C>[OH:6][CH:4]([CH2:3][O:2][CH3:1])[CH2:5][NH:12][CH2:11][C:10]([O:9][CH2:7][CH3:8])=[O:13]

참가 물질

4

반응물 2

HCID 12176Glycine ethyl esterHCID 135891,2-Epoxy-3-methoxypropane

생성물 1

HCID 21922545Ethyl 2-(2-hydroxy-3-methoxypropylamino)acetate수율 100%

시약·촉매·용매 1

HCID 702Ethanol용매

실험 절차

A solution of glycidyl methyl ether (1.00 g) and glycine ethyl ester (5.91 g) in ethanol was stirred overnight, and concentrated under reduced pressure to obtain the title compound (2.17 g).

후처리

  1. concentrationconcentrated under reduced pressure

출처 및 근거

ORD 기록
ord-edab49c1d541455f9a05785795fc1b42
출처 데이터셋
uspto-grants-2006_10
특허 번호
US07122662B2

연결된 노트

불러오는 중…