4-Acetylpyridine → 2-Propen-1-one, 3-(dimethylamino)-1-(4-pyridinyl)-

HRID 1247960노트

반응식

HRID 1247960 반응식
[C:1]([C:4]1[CH:9]=[CH:8][N:7]=[CH:6][CH:5]=1)(=[O:3])[CH3:2].C(O[CH:18](OCC1C=CC=CC=1)[N:19]([CH3:21])[CH3:20])C1C=CC=CC=1>C1C=CC=CC=1>[CH3:18][N:19]([CH3:21])[CH:20]=[CH:2][C:1]([C:4]1[CH:9]=[CH:8][N:7]=[CH:6][CH:5]=1)=[O:3]

참가 물질

4

반응물 2

HCID 142824-AcetylpyridineHCID 748371,1-Bis(benzyloxy)trimethylamine

생성물 1

HCID 7145312-Propen-1-one, 3-(dimethylamino)-1-(4-pyridinyl)-

시약·촉매·용매 1

HCID 241Benzene용매

실험 절차

A mixture of 0.10 mole of 4-acetylpyridine and 0.12 mole of N,N-dimethylformamide dibenzylacetal in benzene was refluxed for 8 hours, giving 3-dimethylamino-1-(4-pyridinyl)-2-propen-1-one.

후처리

  1. temperaturewas refluxed for 8 hours

출처 및 근거

ORD 기록
ord-f1d28c0bd68a4738905a0332c1d8d1f9
출처 데이터셋
uspto-grants-1985_06
특허 번호
US04521422

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