Glycine → 2-[(Butan-2-yl)amino]acetic acid

HRID 1248551노트

반응식

HRID 1248551 반응식
[NH2:1][CH2:2][C:3]([OH:5])=[O:4].CO.[CH3:8][C:9]([CH2:11][CH3:12])=O>[Pd].O>[CH:9]([NH:1][CH2:2][C:3]([OH:5])=[O:4])([CH2:11][CH3:12])[CH3:8]

참가 물질

6

반응물 3

HCID 750GlycineHCID 887MethanolHCID 6569Methyl Ethyl Ketone

생성물 1

HCID 428112-[(Butan-2-yl)amino]acetic acid

시약·촉매·용매 2

HCID 23938Palladium촉매HCID 962Water용매

실험 절차

338 g of glycine (4.5 mols), 1.5 liters of methanol, 15 g of 10% Pd on C, wet with water, and 500 g of methylethylketone (6.93 mols) are charged into the autoclave.

출처 및 근거

ORD 기록
ord-0e503d9cabf14a2ca3a5523662e552cc
출처 데이터셋
uspto-grants-1985_06
특허 번호
US04525294

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