Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Ethyl chloroformate → ethyl N-cyclohexyl-N-[2-[cyclohexyl(ethoxycarbonyl)amino]ethyl]carbamate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Ethyl chloroformate | HCID 10928 | — |
| 반응물 | Sodium Hydroxide | HCID 14798 | — |
| 반응물 | N,N'-Dicyclohexyl-1,2-ethanediamine | HCID 273886 | — |
| 용매 | Chloroform | HCID 6212 | — |
| 생성물 | ethyl N-cyclohexyl-N-[2-[cyclohexyl(ethoxycarbonyl)amino]ethyl]carbamate | HCID 332259 | — |
반응 단계
The N,N'-dicyclohexyl-N,N'-bis(ethoxycarbonyl)-ethylenediamine (m.p. 108° C.) is prepared by reacting N,N'-dicyclohexylethylenediamine with ethyl chlorocarbonate in chloroform at 10°-20° C. in the presence of aqueous NaOH. The obtained product has a purity of 99.7% and is used directly.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04525503 |
| 출처 데이터셋 | uspto-grants-1985_06 |
| ORD ID | ord-138224ee8a414990ab6a30b9ff858b1e |
| 출처 메모 | uspto-grants-1985_06 |