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HRID1248658

反应详情

EQUATION

反应方程式

HRID 1248658 的结构方程式

REACTANTS

反应物

3
结构：CCOC(=O)Cl
HCID10928

Ethyl chloroformate

C3H5ClO2

结构：[Na+].[OH-]
HCID14798

Sodium Hydroxide

HNaO

结构：C1CCC(NCCNC2CCCCC2)CC1
HCID273886

N,N'-Dicyclohexyl-1,2-ethanediamine

C14H28N2

PRODUCTS

生成物

1
结构：CCOC(=O)N(CCN(C(=O)OCC)C1CCCCC1)C1CCCCC1
HCID332259

ethyl N-cyclohexyl-N-[2-[cyclohexyl(ethoxycarbonyl)amino]ethyl]carbamate

C20H36N2O4

AUXILIARIES

试剂、催化剂与溶剂

1
结构：ClC(Cl)Cl
溶剂HCID6212

Chloroform

CHCl3

PROCEDURE

实验过程

The N,N'-dicyclohexyl-N,N'-bis(ethoxycarbonyl)-ethylenediamine (m.p. 108° C.) is prepared by reacting N,N'-dicyclohexylethylenediamine with ethyl chlorocarbonate in chloroform at 10°-20° C. in the presence of aqueous NaOH. The obtained product has a purity of 99.7% and is used directly.

WORKUP

后处理

  1. customat 10°-20° C.