홈MCP워크벤치Skills
홈워크벤치알림마이페이지
llms.txt · MCP 가이드개인정보처리방침 · 이용약관 · 지원v1.8.0
  1. 홈
  2. /반응

Methanol → HCID 178457302, 화합물

HRID 1249117
노트
인쇄 미리보기

반응식

HRID 1249117 반응식
[CH2:1]([NH:4][CH2:5][CH2:6][CH3:7])[CH:2]=[CH2:3].[C:8](=[S:10])=S.C[OH:12]>C(OCC)C>[CH2:1]([NH:4][CH2:5][CH2:6][CH3:7])[CH:2]=[CH2:3].[CH2:1]([N:4]([CH2:5][CH2:6][CH3:7])[C:8](=[S:10])[OH:12])[CH:2]=[CH2:3]
참가 물질실험 절차출처 및 근거반응 노트

참가 물질

5

반응물 3

HCID 887MethanolHCID 6348Carbon DisulfideHCID 12397185Allylpropylamine

생성물 1

HCID 178457302HCID 178457302, 화합물

시약·촉매·용매 1

HCID 3283Diethyl Ether용매

실험 절차

A quantity of N-Allyl-n-propylamine (12.7 g of a 35% solution in methanol, 0.042 mole) was dissolved in 50 ml of ethyl ether, plus 1.52 g of carbon disulfide (0.02 mole) was charged into a beaker and the reaction mixture in the beaker was allowed to let stand for approximately 15 minutes, after which time the volatiles were stripped off, leaving behind 3.7 g of a solid residue, which was identified by conventional instrumental techniques as being the subject compound.

출처 및 근거

ORD 기록
ord-76e7aa8707fb4a9ea8f0024b9042b478
출처 데이터셋
uspto-grants-1986_12
DOI
10.6084/m9.figshare.5104873.v1
특허 번호
US04629499

반응 노트

불러오는 중…

이 페이지에서참가 물질실험 절차출처 및 근거반응 노트