Toluene → Oleylamine styrene oxide

HRID 1249133

반응식

HRID 1249133 반응식
[B].[CH2:2]([NH2:20])[CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9]/[CH:10]=[CH:11]\[CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH3:19].[CH2:21]1[O:29][CH:22]1[C:23]1[CH:28]=[CH:27][CH:26]=[CH:25][CH:24]=1.C1(C)C=CC=CC=1>O>[CH2:2]([NH2:20])[CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9]/[CH:10]=[CH:11]\[CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH3:19].[CH2:21]1[O:29][CH:22]1[C:23]1[CH:28]=[CH:27][CH:26]=[CH:25][CH:24]=1

참가 물질

6

반응물 4

HCID 1140TolueneHCID 7276Styrene OxideHCID 5356789OleylamineHCID 5462311Boron

생성물 1

HCID 86740542Oleylamine styrene oxide

시약·촉매·용매 1

HCID 962Water용매

실험 절차

A sulfurized, boron-containing, heterocyclic compound is prepared by mixing 12 grams of oleylamine, 9.6 grams of styrene oxide and 200 ml of toluene for 30 minutes at room temperature (25° C.) in a single-necked one-liter round-bottomed flask. The flask is placed in a heating mantle and equipped with a water-cooled condenser. The mixture is heated under.reflux for three hours producing an oleylamine/styrene oxide adduct.

후처리

  1. temperaturecooled condenser
  2. temperatureThe mixture is heated under.reflux for three hours

출처 및 근거

ORD 기록
ord-61a838dc335148f1b2e6d4373291faab
출처 데이터셋
uspto-grants-1986_12
특허 번호
US04629580

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