Chlorosulfonic acid → HCID 15480187, 화합물

HRID 1250462노트

반응식

HRID 1250462 반응식
[O:1]([C:8]1[CH:13]=[CH:12][C:11]([N:14]2[CH:18]=[CH:17][N:16]=[CH:15]2)=[CH:10][CH:9]=1)[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.Cl[S:20]([OH:23])(=[O:22])=[O:21]>C(Cl)(Cl)Cl>[N:14]1([C:11]2[CH:12]=[CH:13][C:8]([O:1][C:2]3[CH:3]=[CH:4][C:5]([S:20]([OH:23])(=[O:22])=[O:21])=[CH:6][CH:7]=3)=[CH:9][CH:10]=2)[CH:18]=[CH:17][N:16]=[CH:15]1

참가 물질

4

반응물 2

HCID 24638Chlorosulfonic acidHCID 183266381-(4-Phenoxyphenyl)-1H-imidazole

생성물 1

HCID 15480187HCID 15480187, 화합물

시약·촉매·용매 1

HCID 6212Chloroform용매

실험 절차

137 mmol of 1-(4-phenoxyphenyl)imidazole are dissolved in 250 ml of chloroform. 190 mmol of chlorosulphonic acid are then added dropwise. The whole is left at 45° C. overnight. After cooling and removal of the solvent by evaporation, the resulting oil is taken up in diethyl ether. The resulting solid is filtered off and dried to yield the expected product.

후처리

  1. temperatureAfter cooling
  2. customremoval of the solvent
  3. customby evaporation
  4. filtrationThe resulting solid is filtered off
  5. customdried

출처 및 근거

ORD 기록
ord-fabf148c68754a6dbcbf2d6965c22220
출처 데이터셋
uspto-grants-2002_01
특허 번호
US06339092B1

반응 노트

불러오는 중…