Hydrochloric Acid → HCID 53977328, 화합물

HRID 1251964노트

반응식

[Cl:1][CH2:2][CH:3]=[CH:4][CH:5]=[O:6].Cl.[C:8](=[O:11])([O-])[O-].[Na+].[Na+].[CH3:14]O>>[Cl:1][CH2:2][CH:3]=[CH:4][CH:5]([O:11][CH3:8])[O:6][CH3:14]

참가 물질

반응물 4

HCID 313Hydrochloric Acid

HCID 887Methanol

HCID 10340Sodium Carbonate

HCID 537074664-Chlorobut-2-enal

생성물 1

HCID 53977328HCID 53977328, 화합물

실험 절차

4-Chloro-1,1-dimethyoxy-2-butene (Reagent K) was prepared by reacting 7.46 g. of 4-chloro-2-butenal with 200 ml. of anhydrous methanol and a catalytic amount of hydrochloric acid. The reaction mixture was stirred at room temperature for 16 hours, neutralized with sodium carbonate, filtered, and concentrated.

후처리

filtrationfiltered
concentrationconcentrated

출처 및 근거

ORD 기록: ord-c1ef55076d594af59f15827669981c1a
출처 데이터셋: uspto-grants-1988_05
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US04741804

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