Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
2-(Trifluoromethyl)acrylic acid → 3-Acetylthio-2-trifluoromethylpropanoic acid
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 2-(Trifluoromethyl)acrylic acid | HCID 587694 | — |
| 반응물 | HCID 178473673 | HCID 178473673 | — |
| 생성물 | 3-Acetylthio-2-trifluoromethylpropanoic acid | HCID 12833014 | — |
반응 단계
A mixture of thiolactic acid (50 g) and 2-(trifluoromethyl)acrylic acid [M. W. Buxton, et al., J. Chem Soc., 366 (1954)] (66 g) is heated on the steam bath for one hour and then stored at room temperature for eighteen hours. The reaction mixture is distilled in vacuo to give 3-acetylthio-2-trifluoromethylpropanoic acid.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04745124 |
| 출처 데이터셋 | uspto-grants-1988_05 |
| ORD ID | ord-460d5ee2dd4142559165013c581f2b6b |
| 출처 메모 | uspto-grants-1988_05 |