Methyl iodide → HCID 20130633, 화합물

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[Cl:1][C:2]1[CH:10]=[C:9]([F:11])[C:8]([N:12]2[C:17](=[O:18])[C:16]3[CH2:19][CH2:20][CH2:21][C:15]=3[N:14]([CH3:22])[C:13]2=[O:23])=[CH:7][C:3]=1[C:4]([O-:6])=[O:5].[Na+].[CH3:25]I>>[Cl:1][C:2]1[CH:10]=[C:9]([F:11])[C:8]([N:12]2[C:17](=[O:18])[C:16]3[CH2:19][CH2:20][CH2:21][C:15]=3[N:14]([CH3:22])[C:13]2=[O:23])=[CH:7][C:3]=1[C:4]([O:6][CH3:25])=[O:5]

참가 물질

반응물 2

HCID 6328Methyl iodide

HCID 23687600HCID 23687600, 화합물

생성물 1

HCID 20130633HCID 20130633, 화합물

실험 절차

using sodium 2-chloro-4-fluoro-5-(1,2,4,5,6,7-hexahydro-1-methyl-2,4-dioxo-3H-cyclopenta[d]pyrimidin-3-yl)-benzoate and methyl iodide there is obtained methyl 2-chloro-4-fluoro-5-(1,2,4,5,6,7-hexahydro-1-methyl-2,4-dioxo-3H-cyclopenta[d]pyrimidin-3-yl)-benzoate, m.p. 138°-141° C.

출처 및 근거

ORD 기록: ord-3de3a4e77db44113adeb82244cb772b6
출처 데이터셋: uspto-grants-1988_05
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US04746352

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