Methylhydrazine → Ethyl 2-(1-methylhydrazinyl)acetate

HRID 1254477노트

반응식

[CH3:1][NH:2][NH2:3].Br[CH2:5][C:6]([O:8][CH2:9][CH3:10])=[O:7]>>[CH3:1][N:2]([CH2:5][C:6]([O:8][CH2:9][CH3:10])=[O:7])[NH2:3]

참가 물질

반응물 2

HCID 6061Methylhydrazine

HCID 7748Ethyl bromoacetate

생성물 1

HCID 20288078Ethyl 2-(1-methylhydrazinyl)acetate수율 77.2%

실험 절차

According to the procedure described in the synthesis method of Compound XV-1 with the modification that the reaction was carried out overnight, methylhydrazine 7.13 ml (150 mmol) was reacted with ethyl 2-bromoacetate 16.7 g (100 mmol) to obtain the title compound 10.2 g (77%).

후처리

customdescribed in the synthesis method of Compound XV-1 with the modification that the reaction

출처 및 근거

ORD 기록: ord-186cc4c135604f159249530031554b32
출처 데이터셋: uspto-grants-2013_06
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US08455488B2

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