2,6-Dimethylphenol → HCID 28971738, 화합물

반응식

[CH3:1][C:2]1[CH:15]=[CH:14][CH:13]=[CH:12][C:3]=1[O:4][CH2:5][CH2:6][CH2:7][CH2:8][C:9]([OH:11])=[O:10].[CH3:16]C1C=CC=C(C)C=1O>>[CH3:1][C:2]1[CH:15]=[CH:14][CH:13]=[C:12]([CH3:16])[C:3]=1[O:4][CH2:5][CH2:6][CH2:7][CH2:8][C:9]([OH:11])=[O:10]

참가 물질

반응물 2

HCID 113352,6-Dimethylphenol

HCID 289716655-(2-Methylphenoxy)pentanoic acid

생성물 1

HCID 28971738HCID 28971738, 화합물

실험 절차

5-(2,6-Dimethylphenoxy)pentanoic acid 26c was prepared in the same manner as 26b, except that 2,6-dimethylphenol was used as the starting material. 1H NMR: (400 MHz, CDCl3): 7.0-7.1 (m, 3H), 3.83 (t, 2H, J=6 Hz), 2.37 (t, 2H, J=6 Hz), 2.73 (s. 6H), 1.92 (m, 4H). MS (ESI): 223 [M+H]+; 245 [M+Na]+.

출처 및 근거

ORD 기록: ord-4610f6f4060e4bcb8d2a00561c11ccae
출처 데이터셋: uspto-grants-2013_06
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US08470861B2

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